Extinction coefficients of gold nanoparticles with different sizes were determined by Zetasizer particle analyser and UV ndash;vis absorption spectroscopic measurement. Four different types of gold nanoparticles were prepared and studied: citrate-stabilized nanoparticles in two different sizes; ionic liquid-protected gold nanoparticles and CTAB-protected gold nanoparticles. A linear relationship between the logarithms of extinction coefficients and core diameters of gold particles was found ...
The as-prepared and heat treated iron/cobalt nanoparticles were obtained by iron chloride hexahydrate (FeCl3.6H1O) and cobalt chloride hexahydrate (FeCl3.6H1O) as precursor in the presence of sodium borohydride agent. The samples were characterized by high resolution transmission electron microscopy (HRTEM), field effect scanning electron microscopy (FESEM), X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) in different temperature. XRD pattern of FeCo samples showed ...
An efficient green procedure for the preparation of aryl naphthoxazinones, applying a three-component one-pot condensation reaction of 2-naphthol, aromatic aldehyde and urea in the presence of HA zeolite under heating conditions in dimethyl sulfoxide has been developed. The present procedure offers several advantages such as short reaction time, simple workup and moderate to high yields, recovery and reusability of the catalyst. ...
Denis Howe-Aircraft conceptual design synthesis (2005) ...
Zinc ferrite (Fe2O3/ZnO) nanocomposites were successfully synthesized by simple co-precipitation method via iron (III) nitrate 9-hydrate (Fe(NO3)3.9H2O) and zinc nitrate hexahydrate (Zn(NO3)2.6H2O) as precursor in the presence of cetyltrimethylammonium bromide (CTAB) surfactant. The samples were characterized by high resolution transmission electron microscopy (HRTEM), field effect scanning electron microscopy (FESEM), X-ray diffraction (XRD), X-ray florescence (XRF) and Fourier transform ...
A new bis-Schiff base salophen type Cu(II) complex named as p- bis(3,4-diaminobenzophenimine) phenylenediamine Cu(II) complex, was synthesis via a simple and routine procedure. The desired ligand was prepared through formation of two consecutive imine bond using p-phenylenediamine and 3,4-diaminobenzophenon, followed by reaction with salicylaldehyde and formation of a tetra-dentate ligand. The ligand and its copper complex were characterized step by step with FTIR, 1H NMR, 13C NMR, UV-Vis, CHNS ...
Due to biological and physicochemical properties of poly (-amino acid)s interest in synthesis of their novel derivatives was recently increased. As a new and simple approach, an aromatic poly (-amino acid), poly (AA), was prepared from poly salicylaldehyde (PSA) as a precursor which -amino acid groups formed as pendant groups on the PSA framework. PSA was prepared by a poly condensation reaction, after treatment of salicylaldehyde with chloromethylene group. Transformation of PSA to poly (AA) ...
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